Course Overview
|
Course Synopsis
|
This course is developed to enable the students with fundamental concepts and techniques used in Analytical Chemistry.
|
Course Learning Outcomes
|
To acquaint students with key analytical chemistry concepts involving identification and analysis at the molecular level by introducing a variety of analytical chemistry techniques and their applications at the molecular level.
- Explain the theoretical principles of selected instrumental methods within electro analytical and spectrometric/spectrophotometric methods, and main components in such analytical instruments.
- Explain the theoretical principles of various separation techniques in chromatography, and typical applications of chromatographic techniques.
- Assess and suggest a suitable analytical method for a specific purpose, and evaluate sensitivity, important sources of interferences and errors, and also suggest alternative analytical methods for quality assurance.
- Performing risk assessment of chemical experiments and chemical analytical activity.
- Performing classical analytical experiments, and make observations and assessments of important factors that could affect the analytical result
|
Course Calendar
|
|
|
Week 01
|
1
|
Introduction to analytical chemistry
|
|
2
|
Steps Involved in Chemical Analysis of an Analyte
|
|
3
|
Analyte Separation Techniques
|
|
4
|
Spectroscopic Techniques for Qualitative and Quantitative evaluation of an Analyte
|
|
5
|
Introduction to Chemometrics
|
|
6
|
Chemometrics I: Calculating Mean, Median and Mode
|
|
7
|
Chemometrics II: Understanding Error and Accuracy in Statistical Sense
|
|
8
|
Chemometrics III: Types of Statistical Errors
|
|
9
|
Chemometrics IV: Sources of Statistical Errors
|
Week 02
|
10
|
Chemometrics V: Ways to Remove Statistical Errors
|
|
11
|
Chemometrics VI: How to treat Random Errors
|
|
12
|
Chemometrics VII: Standard Deviation & Confidence Interval
|
|
13
|
Chemometrics VIII: Reporting Analytical Results by Significant Figures
|
|
14
|
Chemometrics IX: Ways to Choose Significant Figures
|
|
15
|
Chemometrics X: ANOVA: Analysis of Variance
|
|
16
|
Chemometrics XI: Standard Preparation of Solutions
|
|
17
|
Chemometrics XII: Goals of Sampling and Sample Preparation
|
Week 03
|
19
|
Quality Control Tools Introduction
|
|
20
|
Quality Control Tools-I: Scatter Diagram
|
|
21
|
Quality Control Tools-II: Cause and Effect Diagram
|
|
22
|
Quality Control Tools-III: Histogram
|
|
23
|
Quality control Tools-IV: Check Sheets
|
|
24
|
Quality control Tools-V: Control Chart
|
|
25
|
Quality control Tools: Graphical Representation of Data
|
|
26
|
Quality control Tools VI: Pareto Diagram
|
|
27
|
Quality Control Tools VII: Stratification
|
Week 04
|
28
|
Quality Control Tools: Excel Worksheet
|
|
30
|
Quality Assurance II: Method Validation
|
|
31
|
Quality assurance III: Linearity
|
|
32
|
Quality assurance IV: Range
|
|
36
|
Quality assurance VIII
|
Week 05
|
41
|
Quality Assurance XIII: Management System
|
|
42
|
Quality Assurance-XIV: Document Control
|
|
43
|
Quality Assurance-XV: Review of Request Tenders & Contracts
|
|
44
|
Quality assurance-XVI: Purchasing Services & Supplies
|
|
45
|
Quality Assurance-XVII: Control of Non-Conforming Testing & Calibration
|
|
46
|
Quality Assurance-XVIII: Corrective Action & Preventive Action
|
Week 06
|
47
|
Quality Assurance-XIX: Control of Records
|
|
48
|
Quality assurance-XX: Internal Audits & Management
|
|
49
|
Quality Assurance-XXI: Review of Technical Clauses
|
|
50
|
Quality assurance-XXII: Test & Calibration Methods, Method Validation
|
|
51
|
Quality Assurance XXIII: Equipment and Measurement Traceability
|
|
52
|
Quality Assurance XXIV: Sampling, Handling and Reporting the Results
|
|
53
|
Chemical Analysis-I: Classical Analytical Methods
|
|
54
|
Chemical analysis-II: Dissociation Constant of a Weak Acid
|
|
55
|
Chemical Analysis-III: Potentiometric Titration Curves
|
Week 07
|
56
|
Chemical Analysis-IV: Chemistry of Acid Base Indicators
|
|
57
|
Chemical Analysis-V: Redox Reactions
|
|
58
|
Chemical Analysis-VI: Complexometric Titrations
|
|
59
|
Chemical Analysis-VII: Indicators used in Complexometric Titrations
|
|
60
|
Chemical Analysis-VIII: Masking and De-masking agents
|
|
61
|
Chemical Analysis-IX: Gravimetric Analysis
|
|
62
|
Chemical Analysis X: Chemistry of Colloids
|
|
63
|
Chemical Analysis-XI: Peptization of Colloids
|
|
64
|
Instrumentation: Chromatography-I
|
Week 08
|
65
|
Chromatography-II: Stationary Phases
|
|
66
|
Chromatography-III: Paper Chromatography
|
|
67
|
Chromatography-IV: Thin Layer Chromatography
|
|
68
|
Chromatography-V: Column Chromatography
|
|
69
|
Chromatography-VI: Electrophoresis
|
|
70
|
Chromatography-VII: High Performance Liquid Chromatography
|
|
71
|
Chromatography-VIII: HPLC Column
|
|
72
|
Chromatography-IX: Types of Chromatography
|
|
73
|
Chromatography X: Method Development on HPLC
|
|
74
|
Chromatography XI: Gas Chromatography
|
|
75
|
Instrumentation: Solvent Extraction-I
|
|
76
|
Instrumentation: Solvent Extraction-II
|
|
77
|
Instrumentation: Solvent Extraction-III
|
|
78
|
Instrumentation: Solvent Extraction-IV
|
Week 09
|
79
|
Instrumentation: Solvent Extraction V
|
|
80
|
Instrumentation: Solvent Extraction-VI
|
|
81
|
Instrumentation: Solid Phase Extraction-I
|
|
82
|
Solid Phase Extraction-II: Polar Sorbent
|
|
83
|
Solid Phase Extraction-III: Non Polar Sorbent
|
|
84
|
Solid Phase Extraction-IV: Ion Exchange Sorbent
|
|
85
|
Solid Phase Extraction-V: Copolymeric Sorbent
|
Week 10
|
87
|
UV-Spectroscopy-II: Wavelength and Energy Relation
|
|
88
|
UV-Spectroscopy-III: Possible Transitions of an Organic molecule
|
|
89
|
UV-Spectroscopy-IV: Why Molecules display color?
|
|
90
|
UV-Spectroscopy-V: Chromophores & Auxochromes
|
|
91
|
UV-Spectroscopy-VI: Beer Lambert’s Law
|
|
92
|
UV-Spectroscopy-VII: Relation between Absorbance & Transmittance
|
|
93
|
UV-Spectroscopy-VIII: UV Spectrophotometer
|
|
94
|
UV-Spectroscopy-IX: Monochromators used in UV Spectrophotometer
|
Week 11
|
95
|
UV-Spectroscopy-X: Photomultiplier Tubes (PMTs)
|
|
96
|
UV-Spectroscopy-XI: Woodward-Fieser Rule for Conjugated Dienes
|
|
97
|
UV-Spectroscopy-XII: Woodward-Fieser Rule for Unsaturated Carbonyl compounds
|
|
98
|
UV-Spectroscopy-XIII: Applications of UV Spectroscopy 1
|
|
99
|
UV-Spectroscopy-XIV: Applications of UV Spectroscopy 2
|
|
101
|
IR-Spectroscopy-II: Vibrational Frequency
|
|
102
|
IR-Spectroscopy-III: Appearance of masses in IR Spectra
|
|
103
|
IR-Spectroscopy-IV: Properties of IR Spectra
|
|
104
|
IR-Spectroscopy-V: Factors influencing IR Absorption 1
|
Week 12
|
105
|
IR-Spectroscopy-VI: Factors influencing IR Absorption 2
|
|
106
|
IR-Spectroscopy-VII: Interpretation of IR Spectra
|
|
107
|
IR-Spectroscopy-VIII: IR Spectrophotometer
|
|
108
|
IR-Spectroscopy-IX: Applications of IR Spectroscopy-1
|
|
109
|
IR-Spectroscopy-X: Applications of IR Spectroscopy-2
|
|
110
|
Atomic Spectroscopy-I
|
|
111
|
Atomic Spectroscopy-II: Hydrogen Spectral lines
|
|
112
|
Atomic Spectroscopy-III: Atomic Absorption Spectroscopy
|
Week 13
|
113
|
Atomic Spectroscopy-IV: Hollow Cathode Lamp
|
|
114
|
Atomic Spectroscopy-V: Nebulizers
|
|
115
|
Atomic Spectroscopy-VI: Atomizers
|
|
116
|
Atomic Spectroscopy-VII: Flame Atomization
|
|
117
|
Atomic Spectroscopy-VIII: Graphite Furnace Atomizer
|
Week 14
|
118
|
Atomic Spectroscopy-IX: Spectral Interferences
|
|
119
|
Atomic Spectroscopy-X: Non-Spectral Interferences
|
|
120
|
Atomic Spectroscopy-XI: Chemical Interferences
|
|
121
|
Atomic Spectroscopy-XII: Ionization Interferences
|
|
122
|
Atomic Spectroscopy-XIII: Atomic Emission Spectroscopy
|
|
123
|
Atomic Spectroscopy-XIV: Sample preparation for Atomic Florescence Spectroscopy
|
|
|
|